Credit will be given for strict adherence to the instructions, for observations precisely recorded, and for accurate inferences. All tests, Observations, and inferences must be clearly entered in your answer book, in ink, at the time they are made. Carry out the following exercises on sample C.

Record your observations and identify any gases evolved 

 

(a) Put all of C into a test tube and add about 5cm\(^3\) of water. Shake the mixture and filter. Keep both the residue and the filtrate

 

(b) Divide the filtrate into two portions;

(i)  To the first portion, add a few drops of dilute trioxonitrate (V) acid followed by about 1cm\(^3\) of silver trioxonitrate (V) solution 

(ii) Add excess aqueous ammonia to the mixture in (i) above

(iii) To the second portion, add about 2cm\(^3\) of dilute sodium hydroxide solution and warm gently

 

(c) Add about 2cm\(^3\) of dilute hydrochloric acid to the residue from (a) above and warm gently. Filter if necessary and divide the resulting solutio into two portions.

(i) To the first portion add dilute sodium hydroxide solution in drops until it is in excess

(ii) To the second portion, add aqueus ammonia in drops until it is in excess.