All your burette readings (initial and final), as well as the size of your pipette, must be recorded but on no account of experimental procedure is required. All calculations must be done in your answer book.

A is 0.50 mol dm\(^{-3}\) hydrochloric acid. B is 0.025 mol dm\(^{-3}\) of a trioxocarbonate (IV) salt.

(a) Put A into the burette and titrate with 20.0cm\(^{-3}\) or 25.0 cm\(^{-3}\) portions of B using methyl orange or screened methyl Orange indicator. Record the volume of your pipette. Tabulate your burette readings and calculate the average of A used.

(b) From your results, calculate the mole ratio of acid to trioxocarbonate (IV)  in the reaction, expressing your answer as a whole number ratio of one.

(c) Given that B contains 7.2g dm\(^{-3}\) of the hydrated trioxocarbonate (IV) salt, calculate the:

(i) concentration of anhydrous salt in B in g dm\(^{-3}\) [Molar mass of anhydrous salt in B = 106g]

(ii) percentage of water of crystallization in the hydrated salt.

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